The Kinetics of Ethanol Volume Change With Variation of Input Volume and Heating Temperature in The Re-Distillation Process of Glucomannan Extraction Residue Using Batch Distillator
DOI:
https://doi.org/10.23960/jtep-l.v11i1.161-173Abstract
Ethanol is commonly used as a solvent in extracting glucomannan from Porang. However, the extraction process often leaves ethanol. The remaining ethanol can be re-distilled to save the use of it. The remaining ethanol is used in the re-distillation process with input volumes of 50L and 100L with variations in heating temperatures of 80°C, 85°C, and 90°C. This study aimed to analyze the effect of the ethanol input volume and temperature on the output volume of re-distilled ethanol and determine the constant change in volume of re-distilled ethanol using kinetics and Arrhenius equations. The results showed that the input volume and heating temperature variation differed significantly from the ethanol output volume. The k value changes in the ethanol output volume from re-distillation with an input volume of 50L and a temperature variation of 80°C, 85°C, and 90°C respectively were 0.0016, 0.0023, and 0.0027 L/min, while the input volume of 100L was 0.0009, 0.001, and 0.0014 L/min. The results of the k value as a function of temperature using the Arrhenius equation showed that the re-distillation process with an input volume of 50L and 100L produces activation energy (Ea) of 55.83 kJ/mol and 46.94 kJ/mol, while the collision frequency value (A) of 3.03x105/min and 7.7x103/min.
Keywords: Distillation, ethanol, glucomannan, arrhenius model, re-distillation
References
Akesowan, A., 2002. Viscosity and Gel Formation of a Konjac Flour from Amorphophallus oncophyllus. AU J. Technol. 5.
Anindita, F., Bahri, S., Hardi, J., 2016. Ekstraksi dan Karakterisasi Glukomanan dari Tepung Biji Salak (Salacca edulis Reinw.). Kovalen 2. https://doi.org/10.22487/j24775398. 2016.v2.i2.6720
Desi, A., Widjanarko, S.B., 2010. Effects of Multiple Ethanol Leaching with Difference Concentration on Physichal and Chemical Properties of Porang Flour (Amorphophallus oncophyllus). https://doi.org/10.13140/RG.2.1.3850.0083
Erawati, E., 2008. Pemurnian Etanol dengan Metode Saline Extractive Distillation. Universitas Muhamadiyah Surakarta.
Gita, A.C., Haryanto, A., Saputra, T.W., Telaumbanua, M., 2018. Penentuan Nilai Parameter Kinetika Orde Satu pada Sintesis Biodiesel dari Minyak Jelantah. J. Tek. Pertan. Lampung J. Agric. Eng. 7, 72. https://doi.org/10.23960/jtep-l.v7i2.72-79
Komariah, L.N., Ramdja, A.F., Leonard, N., 2009. Tinjauan Teoritis Perancangan Kolom Distilasi untuk Pra-Rencana Pabrik Skala Industri. Semantic Sch.
Panggabean, S., 2011. Analisis Kinetika Reaksi Transesterifikasi Pada Produksi Biodiesel Secara Katalitik Dengan Static Mixing Reactor (Tesis). Institut Pertanian Bogor, Bogor.
Setiawan, T., 2018. Rancang Bangun Alat Destilasi Uap Bioetanol dengan Bahan Baku Batang Pisang. J. Media Teknol. 4.
Sönmez, Ö., Yıldız, Ö., Çakır, M.Ö., Gözmen, B., Giray, E.S., 2018. Influence of the addition of various ionic liquids on coal extraction with NMP. Fuel 212, 12–18. https://doi.org/10.1016/j.fuel.2017.10.017
Suryani, N.C., Permana, D.G.M., Jambe, A.G.A., 2016. Pengaruh Jenis Pelarut Terhadap Kandungan Total Flavonoid dan Aktivitas Antioksidan Ekstrak Daun Matoa (Pometia pinnata). Itepa J. Ilmu Dan Teknol. Pangan 5.
Syaflan, M., 2016. Supplementation of Prebiotic Iles-Iles as a Source of Carbon in the MRS Media For Growth of Lactobacillus casei 6.
Usman, B., Dwinanda, L., 2013. Strategi Pemasaran Bioetanol dan Pemanfaatan Limbah Industri Bioetanol. Kementerian Pendidikan dan Kebudayaan.
Verdiana, M., Widarta, I.W.R., Permana, I.D.G.M., 2018. Pengaruh Jenis Pelarut pada Ekstraksi Menggunakan Gelombang Ultrasonik Terhadap Aktivitas Antioksidan Ekstrak Kulit Buah Lemon (Citrus limon (Linn.) Burm F.). J. Ilmu Dan Teknol. Pangan ITEPA 7, 213. https://doi.org/10.24843/itepa.2018.v07.i04.p08
Yanti, A., Mursiti, S., Widiarti, N., Nurcahyo, B., 2019. Optimalisasi Metode Penentuan Kadar Etanol dan Metanol pada Minuman Keras Oplosan Menggunakan Kromatografi Gas (KG) 7.
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